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化学分析仪器质谱液质联用(LC-MS)

实验室LC-MS/MS(TQ-9001)仪器

供应商:
江苏博驰智能科技有限公司
企业类型:
其他

产品简介

博驰智能液质三重四极(TQ)质谱产品包括用于样品分析的液相色谱、三重四极杆质谱仪

详细信息

博驰智能液质三重四极(TQ)质谱产品包括用于样品分析的液相色谱、三重四极杆质谱仪。
 
将每一种分析方法优化到实现分析物的色谱分离、高灵敏度检测和分析。安益谱液质联用控制软件帮助用户节约样品序列设置、提交、下发和运行时间,使用户能够快速运用。
 
LCMSMS  TQ-9001产品特性
 
离子源
 
ESI/APCI快速切换、智能识别
 
即插即用、气电自动对接安装
 
90°直角喷雾、抗污染能力强.
 
质量分析器
 
串联金属四极杆设计,无限接近四极杆理论电场
 
前后预杆,有效平衡离子入射角度,消除边缘场效应.
 
碰撞反应池
 
180°碰撞反应池,去除中性粒子干扰
 
具有轴线加速电场,减小MRM通道间串扰
 
组合阵列式碰撞气体控制,保障碰撞反应的高效进行
 
强大的数据采集和分析软件 —— B&C ITECH Chemstation
 
中(英)文操作界面
 
集成仪器控制、调谐校准、数据采集、数据处理等功能

序号 名称/型号/规格 数量 单位 备注
标准配置
1 主机      
1.1 TQ-9001三重四极杆质谱仪 1 含ESI、APCI离子源,集成注射泵、切换阀,一体式差分涡轮分子泵400/300 L/s,前级机械泵40 m3/h
1.2 SPH1299 二元泵 1 二元超高压液相泵组,压力1300 bar,内置在线真空脱气机
1.3 Alias 自动进样器 1 制冷型、标配2个48位样品瓶架
1.4 T190柱温箱 1  
1.5 溶剂柜 1  
1.6 废液底座 1  
1.7 SV40机械泵 1 内含预装泵油1瓶
2.1 B&C ITECH Chemstation
V1.0数据采集软件
1  
2.2 B&C ITECH Chemstation数据处理软件 1  
2.3        
3 外设/附件      
3.1 启动工具包:
 
1 随机工具盒1套;
软件1个;
软件U盘1个;
ESI 调谐液1瓶;
注射泵连接套装1套:
1ml 注射器、 鲁尔接头、PEEK管线、PEEK 接头;
安装搬运工具1套;
真空连接套件:
波纹管1根,KF40 卡箍2个,KF40 中心支架2个
备用密封圈1套:
离子源密封圈4个
QJET前密封圈1个
QJET后密封圈1个
反吹气密封圈1个;
3.2 仪器说明书 1  
3.3 产品合格证、保修卡 1  
3.4        
选配品
1.1 电脑 1  
1.2 打印机 1  
2  
2.1 UPS稳压电源 1  
2.2 氮气发生器 1  
2.3        
4 备品/耗材      
4.1 色谱柱 1  
4.2 样品瓶 1  
4.3 样品瓶盖 1  

B&C ITECH TQ9001 Triple Quad LC-MS/MS System 
 
Instrument Specifications
 
 Instrument Specification-Mass spectrometer (Triple Quadruple)
Mass range(m/z) 5-2000 amu
Scan speed >10,000 amu/sec
Mass Resolution Unit Resolution FWHM,0.6-0.8 amu
Mass stability ± 0.1Da in 24 hours
Sensitivity MRM mode ESI+, Reserpine 1 pg on column, MRM609/195,S/N > 200,000
Repeatability ESI+, Tacrolimus 5pg on column with 10 injections, Peak area RSD <
1.5%, Retention time RSD<0.25
Scan types Full scan MS and selected ion for both Q1 and Q3, product ion scan, precursor ion scan, neutral loss or gain scan, Multiple reaction
monitoring (MRM)
Dynamic range 6 orders of magnitude
Ionization source Ion Source housing with ESI Probe or APCI probe (max temp: 750ºC) ESI flow rate range: 5 μL/min to 3 mL/min
APCI flow rate range: 200 µL/min to 3 mL/min
Software B&C ITECH Chemstation V1.0
 Instrument Specification-Liquid Chromatograph (UHPLC)
Flow rate range 0.001 - 2.00 ml/min, 0.001 ml/min increments
Pressure range 0-1300 bar
Flow precision ≤ 0.075 % RSD or 0.005 min SD, whichever is greater, H2O in a flow
range of 0.200 - 2.000 mL/min
Flow accuracy ± 1% or ± 10 μL/min, whichever is greater, H2O in a flow range of
0.200 - 2.000 mL/min
Gradient composition
range
0 - 99% (A in B)
Gradient composition
accuracy
± 0.5 % absolute from 5 - 95%, H2O in a flow range of 0.200 - 2.000
mL/min
Gradient composition
precision
≤ 0.15% or 0.01 min SD, whichever is greater, H2O in a flow range of
0.200 - 2.000 mL/min
Injection modes Full loop, partial loopfill and µL pickup mode
Injection volume Programmable from 0 uL-100 uL,1 µL increments
Reproducibility RSD £ 0.3% for full loop injections

  RSD £ 0.5% for partial loopfill injections, injection volumes > 5 µL at constant pressure
RSD £ 1.0% for µL pickup injections, injection volumes > 5 µL
Carry-over < 0.05% with programmable needle wash
Viscosity range 0.1 - 5 cP
Sample tray cooling Built-in Peltier cooling Range: 4°C to Ambient - 3°C
Temp: air temperature in sample compartment: 4°C ± 2°C (at
temperature sensor) (Temperature at relative humidity of 80% and ambient temperature of 25°C)
Needle wash Inside and outside needle wash with drying. Wash can be programmed
between injections and between vials/wells.
Sample capacity Microtiter plates: 2
Vials: 2x 48 (1.5 mL) – optional
Microtiter plates according to SBS standards. 96-well high and low and 384-well.
Column Oven
Temperature control mode
air circulation with heating module
Temperature range ambient+5°C - 60°C, with 1°C increments
Temperature stability Better than 0.1 °C
Column capacity Maximum 2 column, Length150 mm

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